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KMID : 0881720090240010056
Journal of Food Hygiene and Safety
2009 Volume.24 No. 1 p.56 ~ p.62
Monitoring of Patulin Levels in Fruit Juices and Beverages
Eom Joon-Ho

Byun Jung-A
Park You-Gyoung
Seo Eun-Chae
Lee Eun-Mi
Kim Mi-Ra
Sun Nam-Kyu
Kim Chang-Soo
Jung Woo-Young
Jeong Rae-Seok
Na Mi-Ae
Lee Jin-Ha
Abstract
Patulin, a mycotoxin mainly produced by Penicillium and Aspergillus, is found in various foods. In the present, a maximum acceptable level for patulin is established at 50 ¥ìg/kg(ppb) in apple juices and apple concentrates
in Korea. But patulin may be detected in foods produced with other fruits. In the present study, patulin contamination
was analyzed in 520 samples of fruit juices and beverages, and 50 samples of fruit juice concentrates. High
performance liquid chromatography(HPLC) was applied to quantitatively analyze patulin levels in samples and liquid
chromatography-mass spectrometry(LC/MS/MS) was used to remove false positive results. The results showed that
three samples of 520 fruit juices and beverages and five samples of 50 fruit juice concentrates were contaminated by
patulin, 9.8 - 18.0 ¥ìg/kg and 4.7 - 18.2 ¥ìg/kg respectively. Contaminated samples were produced with apple, orange
or pear. This indicates that it is necessary to extend the regulatory range of patulin. In the other hands, the present study
confirmed the effectiveness of LC/MS/MS analytical method to remove false positive results.
KEYWORD
fruit juice, patulin, monitering
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